HRID345182

反应详情

EQUATION

反应方程式

REACTANTS

反应物

$结构：CCCCOC(=O)/C=C\C(=O)OCCCC$

HCID5271569

Dibutyl maleate

C12H20O4

HCID178418558

未命名化合物

PRODUCTS

生成物

结构：CCCCOC(=O)CC(Sc1nnc(SC(CC(=O)OCCCC)C(=O)OCCCC)s1)C(=O)OCCCC

HCID54444250

未命名化合物

CONDITIONS

反应条件

温度: 55 °C

PROCEDURE

实验过程

2,5-Dimercapto-1,3,4-thiadiazole (50.09 g, 0.33 mol) and dibutyl maleate (157.0 g, 0.69 mol) were charged in a reaction flask and heated to 55° C. for 4 hours. The reaction product was filtered warm using filter aid.

WORKUP

后处理

filtrationThe reaction product was filtered
temperaturewarm
filtrationusing filter aid