HRID34525

反应详情

EQUATION

反应方程式

HRID 34525 的结构方程式

PROCEDURE

实验过程

244.8 g of ethyl(2,4-dichloro-5-fluoro-3-nitrobenzoyl)acetate are heated with 166 g of triethyl orthoformate and 185 g of acetic anhydride at 150°-160° C. for 3 hours. The mixture is then concentrated in vacuo, and 270 g of ethyl benzoylethoxyacrylate are obtained as an oily residue.

WORKUP

后处理

  1. concentrationThe mixture is then concentrated in vacuo, and 270 g of ethyl benzoylethoxyacrylate
  2. customare obtained as an oily residue