HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12769229, compound → 8-Oxo-7-(1'-acetoxyethylidene)-2,2-dimethyl-3-oxa-1-azabicyclo[4.2.0]octane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12769229 | HCID 12769229 | — |
| Reactant | 8-Oxo-7-acetoxymethylene-2,2-dimethyl-3-oxa-1-azabicyclo[4.2.0]octane | HCID 53746440 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | 8-Oxo-7-(1'-acetoxyethylidene)-2,2-dimethyl-3-oxa-1-azabicyclo[4.2.0]octane | HCID 54017537 | — |
Reaction Steps
Following the procedure described for the preparation of 8-oxo-7-acetoxymethylene-2,2-dimethyl-3-oxa-1-azabicyclo[4.2.0]octane from 8-oxo-2,2-dimethyl-3-oxa-1-azabicyclo[4.2.0]octane and using N,N-dimethylacetamide instead of N,N-dimethylformamide one obtains 8-oxo-7-(1'-acetoxyethylidene)-2,2-dimethyl-3-oxa-1-azabicyclo[4.2.0]octane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05055573 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-f51203b0dbc846eba89bf38ab5ff062e |
| Source note | uspto-grants-1991_10 |