Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 345358Generated: October 29, 2026

trans 1-Ethoxycarbonyl-2-ethoxycarbonylpyrrolidine-3-ethanol → HCID 86743787, compound

https://huagongshe.com/reaction/345358

Reaction equation

Participants

RoleNameHCIDCharge
Reactanttrans 1-Ethoxycarbonyl-2-ethoxycarbonylpyrrolidine-3-ethanolHCID 86743788—
ReactantHCID 178418287HCID 178418287—
SolventDichloromethaneHCID 6344—
ProductHCID 86743787HCID 86743787—

Reaction Steps

A solution of 0.991 g of trans 1-ethoxycarbonyl-2-ethoxycarbonylpyrrolidine-3-ethanol and 1.24 g pyridinium chlorochromate in 20 ml of methylene chloride is stirred under nitrogen for 4 hours. Mixture is filtered and purified by flash chromatography using ethyl acetate/hexane (1:1) to yield trans 1-ethoxycarbonyl-2-ethoxycarbonylpyrrolidine-3-acetaldehyde.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05057506
Source datasetuspto-grants-1991_10
ORD IDord-cf02b3c29ba74b089a1aebc94bbfc1c3
Source noteuspto-grants-1991_10