HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19992418, compound → HCID 19992420, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19992418 | HCID 19992418 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19992420 | HCID 19992420 | 100.5% |
Reaction Steps
A solution of the product of part (ii) (0.50 g) in methanol (50 ml) was hydrogenated at room temperature and 3.5 bar in the presence of 5% palladium on carbon (50 mg) until the required amount of hydrogen had been absorbed. The catalyst was filtered off and the filtrate was evaporated to give the title compound (0.45 g) as a gum which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05057528 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-7840d8adfc134f738f7fe142192ed012 |
| Source note | uspto-grants-1991_10 |