HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dibenzylhydroxylamine → N-tert-octyl-[3-(N,N-dibenzylaminoxy)-propionamide]
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dibenzylhydroxylamine | HCID 69297 | — |
| Reactant | N-tert-Octylacrylamide | HCID 171970 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | N-tert-octyl-[3-(N,N-dibenzylaminoxy)-propionamide] | HCID 57149163 | — |
Reaction Steps
The procedure of Example I is repeated using 23.31 g of dibenzylhydroxylamine, 1.23 g of potassium-tert-butoxide and 20.0 g of N-tert-octylacrylamide in 100 ml of dry tetrahydrofuran to afford the title compound as a white crystalline solid: mp 96°-98° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05057563 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-5a98df59669f4e07a5cf00f6d0fde8ea |
| Source note | uspto-grants-1991_10 |