Ethanolamine → N-(3,7,11,15-Tetramethyl-2-hexadecenoyl)-ethanolamine

HRID 34555Notes

Reaction equation

[CH3:1][C:2]([CH2:7][CH2:8][CH2:9][CH:10]([CH3:22])[CH2:11][CH2:12][CH2:13][CH:14]([CH3:21])[CH2:15][CH2:16][CH2:17][CH:18]([CH3:20])[CH3:19])=[CH:3][C:4]([OH:6])=O.[CH2:23]([CH2:25][NH2:26])[OH:24]>>[CH3:1][C:2]([CH2:7][CH2:8][CH2:9][CH:10]([CH3:22])[CH2:11][CH2:12][CH2:13][CH:14]([CH3:21])[CH2:15][CH2:16][CH2:17][CH:18]([CH3:20])[CH3:19])=[CH:3][C:4]([NH:26][CH2:25][CH2:23][OH:24])=[O:6]

Participants

Reactant 2

HCID 700Ethanolamine

HCID 134564CID 134564

Product 1

HCID 54155557N-(3,7,11,15-Tetramethyl-2-hexadecenoyl)-ethanolamineYield 95%

Procedure

The procedure of Example 1 was repeated except that 6.2 g of 3,7,11,15-tetramethyl-2-hexadecenoic acid and 1.8 ml of ethanolamine were used as starting materials. 6.7 g (yield 95%) of the title compound was obtained as a colorless oil.

Sources & evidence

ORD record: ord-cbd788cc13b9459e989c02656be8f5c4
Source dataset: uspto-grants-1988_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04762829

Reaction notes

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