Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-Fluorophenol | HCID 9743 | — |
| Reactant | Cyclopropanecarbonyl chloride | HCID 77637 | — |
| Product | HCID 15096980 | HCID 15096980 | 98% |
Reaction Steps
To 31.4 parts of 3-fluorophenol were added dropwise 29.3 parts of cyclopropanecarbonyl chloride at 80° C. Upon completion, the whole was stirred for 1 hour 80° C. The reaction mixture was distilled, yielding 49.7 parts (98%) of (3-fluorophenyl)cyclopropanecarboxylate; bp. 75°-85° C. at 0.5 mm. pressure (intermediate 86).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05057525 |
|---|
| Source dataset | uspto-grants-1991_10 |
|---|
| ORD ID | ord-bf2c4d1ee68048e18c2a690e31fbcc88 |
|---|
| Source note | uspto-grants-1991_10 |
|---|
