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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 345655Generated: October 30, 2026

Ammonia → HCID 5327661, compound

https://huagongshe.com/reaction/345655

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
ReactantHCID 14525670HCID 14525670—
SolventDimethylformamideHCID 6228—
ProductHCID 5327661HCID 5327661—

Reaction Conditions

Temperature130 °C

Reaction Steps

56 mg of 3-(1-methyl-3-indolyl)-4-(1-naphthyl)furan-2,5-dione were treated with 5 ml of DMF and 5 ml of 33% aqueous ammonia and the mixture was heated at 130° C. for 5 hours. The formed precipitate was filtered off, washed with water and dried to give 53 mg of 3-(1-methyl-3-indolyl)-4-(1-naphthyl)-1H-pyrrole-2,5-dione, m.p. 258°-260° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05057614
Source datasetuspto-grants-1991_10
ORD IDord-d0c0af44b91c4a06a3436126548b68d2
Source noteuspto-grants-1991_10