HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 18780224, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | HCID 18780217 | HCID 18780217 | — |
| Solvent | Ammonia | HCID 222 | — |
| Product | HCID 18780224 | HCID 18780224 | — |
Reaction Steps
A solution of 2.50 g of 3-[1-(3-azidopropyl)-3-indolyl]-4-(1-methyl-3-indolyl)furan-2,5-dione in 13 ml of DMF and 18 ml of 33% aqueous ammonia was heated to 140° C. for 4 hours. The product was filtered off from the cooled mixture to give 2.27 g of 3-[1-(3-azidopropyl)-3-indolyl]-4-(1-methyl-3-indolyl)-1H-pyrrole-2,5-dione, m.p. 222°-224° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05057614 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-3e591cf09dae4b68ad1435f81f574031 |
| Source note | uspto-grants-1991_10 |