HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-5-methylisoxazole → Urea, N-(2,6-dimethylphenyl)-N'-(5-methyl-3-isoxazolyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-5-methylisoxazole | HCID 66172 | — |
| Reactant | Isocyanate | HCID 105034 | — |
| Reactant | Tetrahydrofuran toluene | HCID 22635083 | — |
| Product | Urea, N-(2,6-dimethylphenyl)-N'-(5-methyl-3-isoxazolyl)- | HCID 3076190 | 64% |
Reaction Steps
7 g (0.04 mole) of the preceding isocyanate, 4 g (0.04 mole) of 3-amino 5-methyl isoxazole are heated at reflux for 16 h in a toluene THF mixture (100--100 ml). The precipitate formed is filtered off, the solution is concentrated. The crystals are recrystallized from an ethanol-water mixture. M.p.=200° Yield 64%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05059614 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-da7c80cb45cc4c34913e3b085b3ae8ed |
| Source note | uspto-grants-1991_10 |