Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(2-Trimethylsilyl-4-furyl)propan-1-ol → 3-(2-Trimethylsilyl-4-furyl)propan-1-al
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(2-Trimethylsilyl-4-furyl)propan-1-ol | HCID 15037091 | — |
| 반응물 | HCID 178418287 | HCID 178418287 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 3-(2-Trimethylsilyl-4-furyl)propan-1-al | HCID 15037092 | — |
반응 단계
To a stirring mixture of pyridinium chlorochromate (3.89 g, 18.03 mmol) suspended in methylene chloride (100 ml) at 0° was added 3-(2-trimethylsilyl-4-furyl)propan-1-ol (1.19 g. 6.01 mmol), prepared as in Example 2, in dry methylene chloride (15 ml). This mixture was allowed to warm to room temperature, stirred for 90 minutes, filtered and concentrated to give the desired aldehyde.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05059611 |
| 출처 데이터셋 | uspto-grants-1991_10 |
| ORD ID | ord-395fd4e17bc942579f2255cdc7cdaab9 |
| 출처 메모 | uspto-grants-1991_10 |