HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoylacetone → 3-(1-Pyrrolidinyl)crotonophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoylacetone | HCID 7166 | — |
| Reactant | Pyrrolidine | HCID 31268 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 3-(1-Pyrrolidinyl)crotonophenone | HCID 10703898 | 91.2% |
Reaction Steps
To a solution of 17.4 g of benzoylacetone in 100 ml of ethyl acetate is added a solution of 7.35 g of pyrrolidine in 50 ml of ethyl acetate. The reaction mixture is stirred at room temperature for 16 hours. The precipitated compound is collected by filtration to give 20.30 g of 3-(1-pyrrolidinyl)crotonophenone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05059691 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-d522da771bca4d258ebfce37ee653086 |
| Source note | uspto-grants-1991_10 |