3-Fluoro-1,2-propanediol → HCID 19888726, compound

HRID 345973Notes

Reaction equation

HRID 345973 reaction equation
[F:1][CH2:2][CH:3]([CH2:7][CH:8]([F:10])[F:9])[CH:4]([F:6])[F:5].FCC(O)CO>>[F:1][CH2:2][C:3]([CH:7]=[C:8]([F:10])[F:9])=[C:4]([F:6])[F:5]

Participants

3

Reactant 2

HCID 16573-Fluoro-1,2-propanediolHCID 19888727HCID 19888727, compound

Product 1

HCID 19888726HCID 19888726, compound

Procedure

As another example, 2-fluoromethyl-1,1,4,4-tetrafluorobutane may be prepared by oxidizing commercially available 3-fluoro-1,2-propanediol to form a product which may then be reacted with CF2 carbene to form 2-fluoromethyl-1,1,4,4-tetrafluoro-1,3-butadiene which may then be hydrogenated to form 2-fluoromethyl-1,1,4,4-tetrafluorobutane.

Workup

  1. customto form a product which

Sources & evidence

ORD record
ord-170def8c59634aa884708cd7a7b3c8b5
Source dataset
uspto-grants-1991_10
Patent number
US05059728

Reaction notes

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