1,1-bis(Trifluoromethyl)ethane → HCID 19788892, compound

HRID 345981Notes

Reaction equation

HRID 345981 reaction equation
FC(F)C(C(F)(F)F)C(F)(F)F.CC(C(F)(F)F)C(F)(F)F.FC(F)(F)C(CC(F)(F)F)C(F)(F)F.FC(F)(F)C(C(F)(F)CC)C(F)(F)F.FC(F)(F)[CH:53]([C:58]([F:65])([F:64])[C:59]([F:63])([F:62])[CH2:60][CH3:61])C(F)(F)F>>[F:62][C:59]([F:63])([C:58]([F:65])([F:64])[CH3:53])[CH:60]=[CH2:61]

Participants

6

Reactant 5

HCID 27782581,1-bis(Trifluoromethyl)ethaneHCID 150445742-(Difluoromethyl)-1,1,1,3,3,3-hexafluoropropaneHCID 189357151,1,1,4,4,4-Hexafluoro-2-(trifluoromethyl)butaneHCID 19895027HCID 19895027, compoundHCID 19895031HCID 19895031, compound

Product 1

HCID 19788892HCID 19788892, compound

Procedure

The boiling point of 2-difluoromethyl-1,1,1,3,3,3-hexafluoropropane is calculated to be about 38° C. while the boiling point of 2-methyl-1,1,1,3,3,3-hexafluoropropane is calculated to be about 30° C. The boiling point of 2-trifluoromethyl-1,1,1,4,4,4-hexafluorobutane is calculated to be about 75° C. The boiling point of 2-trifluoromethyl-1,1,1,3,3-pentafluoropentane is calculated to be about 38° C. while the boiling point of 2-trifluoromethyl-1,1,1,3,3,4,4-heptafluorohexane is calculated to be about 55° C.

Workup

  1. customto be about 30° C
  2. customto be about 75° C
  3. customto be about 55° C.

Sources & evidence

ORD record
ord-923af8fa0c3a4916be4dbf6c9c02a2a7
Source dataset
uspto-grants-1991_10
Patent number
US05059728

Reaction notes

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