HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 67592306, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | HCID 5146562 | HCID 5146562 | — |
| Product | HCID 67592306 | HCID 67592306 | 63% |
Reaction Steps
By the method of Example 146, 25.0 g (75.5 mmol) of 6-methoxy-1-(p-toluenesulfonyl)-2,3-dihydro-4(1H)quinolinone (J. Am. Chem. Soc., Vol. 71, p. 1901, 1949) and 12.0 g (113 mmol) of benzaldehyde were converted to 20.0 g (63%) of present title product recrystallized from ether-hexane, m.p. 131°-132° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05059609 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-e4196ccf36fd4dc3b344c57ab7e25a21 |
| Source note | uspto-grants-1991_10 |