HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylpyridin-3-ol → HCID 19991522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylpyridin-3-ol | HCID 70719 | — |
| Reactant | HCID 19091476 | HCID 19091476 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 19991522 | HCID 19991522 | — |
Reaction Steps
By the same methods, 2-methyl-3-hydroxypyridine (7.30 g, 0.067 mol) was converted to 1.17 g of 6-benzyloxy-3-(2-methyl-3-pyridyloxy)-4-chromanone [1H-NMR includes delta 2.48 (s, 3H), 4.6 (m, 2H) and 4.93 (dd, 1H); MS includes 361 (M+) and base peak at 91; IR (CHCl3) 1697, 1486 cm-1 ].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05059609 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-3241f3f23ada42be86a4febd06d9267b |
| Source note | uspto-grants-1991_10 |