Nitric Acid → HCID 19990451, compound

Participants

Reaction Conditions

Reaction Steps

20 ml 100% nitric acid was cooled to 0° C. and 2.0 g (6.8 mmol) N-ethoxalyl-3,4,5-trichloroaniline was added. The reaction mixture was stirred at 0° C. for 10 min. and 200 ml ice-water was added. The precipitate was filtered off, washed with water and ethanol to give 1.2 g (52%) of N-ethoxalyl-2-nitro-3,4,5-trichloroaniline. M.p. 84° C.

Provenance & Evidence