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HRID346495

反应详情

EQUATION

反应方程式

HRID 346495 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[Na+].[Na+]
HCID10340

Carbonic acid sodium salt (1:2)

CNa2O3

结构：Fc1cccc(S)c1
HCID75710

m-Fluorobenzenethiol

C6H5FS

结构：Cc1c(Cl)cccc1S(=O)(=O)Nc1nc(C[C@@H](C)OS(=O)(=O)c2cccc(Cl)c2C)ns1
HCID86595861

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c(Cl)cccc1S(=O)(=O)Nc1nc(C[C@@H](C)Sc2cccc(F)c2)ns1
HCID16119014

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

(R)-2-(5-{[(3-chloro-2-methylphenyl)sulfonyl]amino}-1,2,4-thiadiazol-3-yl)-1-methylethyl 3-chloro-2-methylbenzenesulfonate (example 98), 3-fluorothiophenol (1 eq) and sodium carbonate (1 eq) in CH3CN were heated overnight. Standard work-up and purification yielded the desired product.

WORKUP

后处理

  1. customStandard work-up and purification