関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Sodium sulfite heptahydrate | HCID 160916 | — |
| 反応物 | Sodium Bicarbonate | HCID 516892 | — |
| 反応物 | 6-Chloronaphthalene-2-sulfonyl chloride | HCID 10635129 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 23704948 | HCID 23704948 | 96.6% |
反応手順
6-Chloronaphth-2-ylsulphonyl chloride (2.61 g) was added in one portion to a stirred mixture of sodium sulphite heptahydrate (4.71 g), sodium bicarbonate (1.64 g) and water (25 ml) which had been heated to 70° C. The resultant mixture was heated to that temperature for 3 hours and then allowed to cool slowly to ambient temperature. The crystalline precipitate was isolated giving sodium 6-chloronaphth-2-ylsulphinate (2.4 g) which was used without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07173025B1 |
|---|
| 出典データセット | uspto-grants-2007_02 |
|---|
| ORD ID | ord-479b1b54406f4419abd03e4c28b8b5b5 |
|---|
| 出典メモ | uspto-grants-2007_02 |
|---|
