참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sodium sulfite heptahydrate | HCID 160916 | — |
| 반응물 | Sodium Bicarbonate | HCID 516892 | — |
| 반응물 | 6-Bromonaphthalene-2-sulfonyl chloride | HCID 14457741 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Sodium 6-bromonaphthalene-2-sulfinate | HCID 69513058 | 89.5% |
반응 단계
6-Bromonaphth-2-ylsulphonyl chloride (9.4 g) was added in small portions over 3 hours to a stirred mixture of sodium sulphite heptahydrate (14.46 g), sodium bicarbonate (5.08 g) and water (100 ml) which had been heated to 70° C. The resultant mixture was allowed to cool slowly to ambient temperature. The crystalline precipitate was isolated giving sodium 6-bromonaphth-2-ylsulphinate (8.07 g) which was used without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07173025B1 |
|---|
| 출처 데이터셋 | uspto-grants-2007_02 |
|---|
| ORD ID | ord-35a35cf4c9d84bb8a5aa8f09b48f63a4 |
|---|
| 출처 메모 | uspto-grants-2007_02 |
|---|
