4-Butoxybenzenesulfonyl Chloride → HCID 10232281, compound

Participants

Reaction Steps

The compound was synthesized from of N-{2-amino-5-(4-t-butyloxycarbonyl-1,4-diazepan-1-yl)-phenyl}benzenesulfonamide and 4-n-butoxybenzenesulfonylchloride (67 mg, 0.269 mmol) to give 27 mg as purple solid. M+1 559.4 Calcd 559.20; 1HNMR δ 7.77–7.47 (m, 7H), 6.96–6.93 (m, 2H), 6.55 (d, 1H), 6.52 (d, 1H), 6.41 (d, 1H), 4.01 (t, 2H), 3.63 (app t, 2H), 3.43 (app t, 2H), 3.25 (app t, 2H), 3.17 (app t, 2H), 2.11–2.03 (m, 2H), 1.80–1.71 (m, 2H), 1.53–1.45 (m, 2H), 0.98 (t, 3H).

Provenance & Evidence