HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methanesulfonylbenzene-1-sulfonyl chloride → HCID 10121482, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methanesulfonylbenzene-1-sulfonyl chloride | HCID 2735182 | — |
| Reactant | N-(2-amino-5-(4-t-butyloxycarbonyl-1,4-diazepan-1-yl)-phenyl}benzenesulfonamide | HCID 22272501 | — |
| Product | HCID 10121482 | HCID 10121482 | — |
Reaction Steps
The compound was synthesized from of N-{2-amino-5-(4-t-butyloxycarbonyl-1,4-diazepan-1-yl)-phenyl}benzenesulfonamide and 4-methylsulfonylbenzenesulfonylchloride (69 mg, 0.269 mmole) to give 38 mg as purple solid. M+1 565.3 Calcd 565.12; 1HNMR δ 8.08–7.48 (m, 9H), 6.76 (d, 1H), 6.48 (dd, 1H), 6.32 (d, 1H), 3.61 (app t, 2H), 3.21 (app t, 2H), 3.17 (app t, 2H), 3.14 (app t, 2H), 2.08–2.00 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07173035B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-d79d070c77ea4fdfb6bd923a51432920 |
| Source note | uspto-grants-2007_02 |