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HRID34688

反应详情

EQUATION

反应方程式

HRID 34688 的结构方程式

REACTANTS

反应物

2
结构：O=[N+]([O-])O
HCID944

Nitric Acid

HNO3

结构：O=C(Oc1ccc(O)c(-c2ccccc2O)c1)c1ccccc1
HCID22163020

未命名化合物

PRODUCTS

生成物

1
结构：O=C(Oc1ccc(-c2ccc([N+](=O)[O-])cc2)cc1)c1ccccc1
HCID259633

4'-nitrobiphenyl-4-yl benzoate

C19H13NO4

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

CONDITIONS

反应条件

温度
85 °C

PROCEDURE

实验过程

4-Benzoyloxybiphenol (40 g) is mixed with 310 ml of glacial acetic acid and heated to 85° C. Fuming nitric acid (100 ml) is added slowly while maintaining the reaction medium temperature between 85°-90° C. After complete addition, the reaction is cooled to room temperature.

WORKUP

后处理

  1. temperaturewhile maintaining the reaction medium temperature between 85°-90° C
  2. additionAfter complete addition
  3. temperaturethe reaction is cooled to room temperature