참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | m-Chloroperbenzoic acid | HCID 70297 | — |
| 반응물 | 4-(4-Pentenoxy)-4'-nitrobiphenyl | HCID 19901284 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 4-(4,5-Epoxypentoxy)-4'-nitrobiphenyl | HCID 22163019 | — |
반응 단계
To 250 ml of methylene chloride is added 28.3 g of 4-(4-penteneoxy)-4'-nitrobiphenyl. The solution is cooled to 0° C., and 18 g of meta-chloroperbenzoic acid is added slowly. The mixture is stirred at 0° C. for 24 hours, and allowed to warm to room temperature.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04762912 |
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| 출처 데이터셋 | uspto-grants-1988_08 |
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| ORD ID | ord-da473f1399ef46dd87d62d2e9d957784 |
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| 출처 메모 | uspto-grants-1988_08 |
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