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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 34690생성일: 2026년 10월 25일

m-Chloroperbenzoic acid → 4-(4,5-Epoxypentoxy)-4'-nitrobiphenyl

https://huagongshe.com/reaction/34690

반응식

참여 물질

역할이름HCID투입량
반응물m-Chloroperbenzoic acidHCID 70297—
반응물4-(4-Pentenoxy)-4'-nitrobiphenylHCID 19901284—
용매DichloromethaneHCID 6344—
생성물4-(4,5-Epoxypentoxy)-4'-nitrobiphenylHCID 22163019—

반응 조건

온도0 °C

반응 단계

To 250 ml of methylene chloride is added 28.3 g of 4-(4-penteneoxy)-4'-nitrobiphenyl. The solution is cooled to 0° C., and 18 g of meta-chloroperbenzoic acid is added slowly. The mixture is stirred at 0° C. for 24 hours, and allowed to warm to room temperature.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04762912
출처 데이터셋uspto-grants-1988_08
ORD IDord-da473f1399ef46dd87d62d2e9d957784
출처 메모uspto-grants-1988_08