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N-(2-Methoxyethyl)ethylamine → Ethyl-{4-[3-(4-fluoro-phenyl)-benzo[d]isothiazol-6-yloxy]-butyl}-(2-methoxy-ethyl)-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-(2-Methoxyethyl)ethylamine | HCID 546877 | — |
| 反応物 | HCID 22314175 | HCID 22314175 | — |
| 生成物 | Ethyl-{4-[3-(4-fluoro-phenyl)-benzo[d]isothiazol-6-yloxy]-butyl}-(2-methoxy-ethyl)-amine | HCID 22314136 | — |
反応手順
In analogy to example 3.1, 6-(4-Bromo-butoxy)-3-(4-fluoro-phenyl)-benzo[d]isothiazole and N-(2-Methoxyethyl)ethylamine were converted to yield Ethyl-{4-[3-(4-fluoro-phenyl)-benzo[d]isothiazol-6-yloxy]-butyl}-(2-methoxy-ethyl)-amine which was transferred into its salt by treatment with formic acid, MS: 403 (MH+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07173043B2 |
| 出典データセット | uspto-grants-2007_02 |
| ORD ID | ord-10bffcbdfe964c8aab51906f442192c0 |
| 出典メモ | uspto-grants-2007_02 |