HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxybenzenethiol → 2-Methyl-3-(4-trifluoromethyl-phenyl)-benzo[b]thiophen-6-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxybenzenethiol | HCID 84989 | — |
| Reactant | 2-Bromo-1-(4-(trifluoromethyl)phenyl)propan-1-one | HCID 10423819 | — |
| Product | 2-Methyl-3-(4-trifluoromethyl-phenyl)-benzo[b]thiophen-6-ol | HCID 17932879 | — |
Reaction Steps
In analogy to examples 26.1–26.3, 3-Mercaptoanisole and 2-Bromo-1-(4-trifluoromethyl-phenyl)-propan-1-one were converted to yield 2-Methyl-3-(4-trifluoromethyl-phenyl)-benzo[b]thiophen-6-ol as colorless amorphous solid, MS: 308 (M).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07173043B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-9ed1ef29d48844c3b251a86a30960805 |
| Source note | uspto-grants-2007_02 |