Bis(2-Methoxyethyl)amine → {3-[3-(4-Bromo-phenyl)-benzo[b]thiophen-6-yloxy]-propyl}-bis-(2-methoxy-ethyl)-amine

Participants

Role	Name	HCID	Charge
Reactant	Bis(2-Methoxyethyl)amine	HCID 2383	—
Reactant	3-(4-Bromo-phenyl)-6-(3-bromo-propoxy)-benzo[b]thiophene	HCID 22313968	—
Product	{3-[3-(4-Bromo-phenyl)-benzo[b]thiophen-6-yloxy]-propyl}-bis-(2-methoxy-ethyl)-amine	HCID 22314045	—

Reaction Steps

In analogy to example 3.1, 3-(4-Bromo-phenyl)-6-(3-bromo-propoxy)-benzo[b]thiophene and bis(2-methoxyethyl)amine were converted to yield {3-[3-(4-Bromo-phenyl)-benzo[b]thiophen-6-yloxy]-propyl}-bis-(2-methoxy-ethyl)-amine as light brown oil, MS: 478 (MH+, 1Br).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07173043B2
Source dataset	uspto-grants-2007_02
ORD ID	ord-127f8427862044e9b172d1839b1d319e
Source note	uspto-grants-2007_02