Bis(2-Methoxyethyl)amine → {4-[3-(4-Bromo-phenyl)-benzo[b]thiophen-6-yloxy]-butyl}-bis-(2-methoxy-ethyl)-amine

Participants

Role	Name	HCID	Charge
Reactant	Bis(2-Methoxyethyl)amine	HCID 2383	—
Reactant	6-(4-Bromo-butoxy)-3-(4-bromo-phenyl)-benzo[b]thiophene	HCID 22314056	—
Product	{4-[3-(4-Bromo-phenyl)-benzo[b]thiophen-6-yloxy]-butyl}-bis-(2-methoxy-ethyl)-amine	HCID 22314203	—

Reaction Steps

According to the method in example 29, 6-(4-Bromo-butoxy)-3-(4-bromo-phenyl)-benzo[b]thiophene and bis(2-methoxyethyl)amine were converted to yield {4-[3-(4-Bromo-phenyl)-benzo[b]thiophen-6-yloxy]-butyl}-bis-(2-methoxy-ethyl)-amine as light brown oil, MS: 492 (MH+,1Br).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07173043B2
Source dataset	uspto-grants-2007_02
ORD ID	ord-77256fe665444a199fe12179ff03681d
Source note	uspto-grants-2007_02