HCID 22314084, compound → HCID 22313999, compound

HRID 347225Notes

Reaction equation

HRID 347225 reaction equation
[F:1][C:2]([F:27])([F:26])[C:3]1[CH:8]=[CH:7][C:6]([C:9]2[C:13]3[CH:14]=[CH:15][C:16](OS(C(F)(F)F)(=O)=O)=[CH:17][C:12]=3[S:11][N:10]=2)=[CH:5][CH:4]=1.[CH2:28]([N:30]([CH2:35][CH2:36][O:37][CH3:38])[CH:31]([CH3:34])[C:32]#[CH:33])[CH3:29]>>[CH2:28]([N:30]([CH2:35][CH2:36][O:37][CH3:38])[CH:31]([CH3:34])[C:32]#[C:33][C:16]1[CH:15]=[CH:14][C:13]2[C:9]([C:6]3[CH:5]=[CH:4][C:3]([C:2]([F:1])([F:26])[F:27])=[CH:8][CH:7]=3)=[N:10][S:11][C:12]=2[CH:17]=1)[CH3:29]

Participants

3

Reactant 2

HCID 22314084HCID 22314084, compoundHCID 57428077Trifluoro-methanesulfonic acid 3-(4-trifluoromethyl-phenyl)-benzo[d]isothiazol-6-yl ester

Product 1

HCID 22313999HCID 22313999, compound

Procedure

In analogy to example 14.1, Trifluoro-methanesulfonic acid 3-(4-trifluoromethyl-phenyl)-benzo[d]isothiazol-6-yl ester and Ethyl-(2-methoxy-ethyl)-(1-methyl-prop-2-ynyl)-amine were converted to yield Ethyl-(2-methoxy-ethyl)-{1-methyl-3-[3-(4-trifluoromethyl-phenyl)-benzo[d]isothiazol-6-yl]-prop-2-ynyl}-amine as brown oil, MS: 433 (MH+).

Sources & evidence

ORD record
ord-7ff17beeb5f34ae58bc402f37c6df417
Source dataset
uspto-grants-2007_02
Patent number
US07173043B2

Reaction notes

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