Cyclohexene → HCID 21082862, compound

Participants

Reaction Steps

1.5 g (5.63 mmol) of (2,5-dimethylpyrrolidin-1-yl)-3,5-dinitropyridine, obtained according to Protocol A from 2-chloro-3,5-dinitropyridine and 2,5-dimethylpyrrolidine, were reduced by hydrogen transfer in 50 ml of ethanol in the presence of palladium-on-charcoal and 5 ml of cyclohexene. 900 mg of N-(3,5-diaminopyrid-2-yl)-2,5-dimethylpyrrolidine dihydrochloride were obtained.

Provenance & Evidence