HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 10226339, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | N-[3-[2-(diethylamino)ethyl]-1H-indol-5-yl]naphthalene-1-sulfonamide | HCID 10180527 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10226339 | HCID 10226339 | — |
Reaction Steps
1.05 g (2.5 mMol) of N-[3-(2-diethylaminoethyl)-1H-indol-5-yl]naphthalene-1-sulphonamide (example 2) are dissolved in 10 ml of ethanol and 0.6 ml are added of a 4.2 N solution of hydrochloric acid in ethanol. It is allowed to crystallise at ambient temperature. N-[3-(2-diethylaminoethyl)-1H-indol-5-yl]naphthalene-1-sulphonamide hydrochloride is obtained as a solid with m.p.=255–257° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07176200B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-cbe3977f05bf47b7a34318d8f77903d1 |
| Source note | uspto-grants-2007_02 |