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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 348287생성일: 2026년 10월 25일

3-(4-Benzyloxy-3-methoxyphenyl)-2-methyl-2-phenoxypropionic Acid → 3-(4-Hydroxy-3-methoxy-phenyl)-2-methyl-2-phenoxypropionic Acid

https://huagongshe.com/reaction/348287

반응식

참여 물질

역할이름HCID투입량
반응물3-(4-Benzyloxy-3-methoxyphenyl)-2-methyl-2-phenoxypropionic AcidHCID 22339970—
촉매PalladiumHCID 23938—
용매EthanolHCID 702—
생성물3-(4-Hydroxy-3-methoxy-phenyl)-2-methyl-2-phenoxypropionic AcidHCID 22339982—

반응 단계

A solution of 3-(4-benzyloxy-3-methoxyphenyl)-2-methyl-2-phenoxypropionic acid (6.86 g, 17.5 mmol) in EtOH (175 mL) was added to 5% Pd/C (186 mg, 10 wt %). The mixture was purged first with nitrogen, then with H2, which was then applied at 45 p.s.i. for 2 h. Pd/C was subsequently filtered off through celite, and the filtrate was concentrated to a crude oil (5.42 g, in excess of theory). MS (EI) 301.2 (M−H)−.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07176224B2
출처 데이터셋uspto-grants-2007_02
ORD IDord-a91a9e5bcb3e461a9bcc70bfa790c554
출처 메모uspto-grants-2007_02