Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HCID 69353995, 화합물 → 2-(3-Fluorophenoxy)-3-(4-hydroxyphenyl)-2-methyl-propionic acid ethyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | HCID 69353995 | HCID 69353995 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 2-(3-Fluorophenoxy)-3-(4-hydroxyphenyl)-2-methyl-propionic acid ethyl ester | HCID 69315813 | — |
반응 단계
2-(3-Fluorophenoxy-3-(4-benzyloxyphenyl)-2-methyl-propionic acid ethyl ester (2.1 mmol) was dissolved in ethyl acetate (30 mL) and treated with 5% palladium on carbon (300 mg), and stirred under an atmosphere of hydrogen for 20 h. The suspension was filtered rough celite and concentrated in vacuo to an oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07176224B2 |
| 출처 데이터셋 | uspto-grants-2007_02 |
| ORD ID | ord-76809831720740c7ad2f51138dd0741c |
| 출처 메모 | uspto-grants-2007_02 |