HRID348452

反应详情

EQUATION

反应方程式

HRID 348452 的结构方程式

PROCEDURE

实验过程

The titled compound was prepared from [5-(4-fluorophenylcarbamoyl)pyrimidin-2-yloxy]acetic acid using 2-(2,5-dimethylpyrrol-1-yl)pyridin-3-ol (32 mg, 0.17 mmol) as the source alcohol. Chromatographic (30–40% ethyl acetate/hexane) purification yielded 22 mg (28%) of the titled compound. ESI-MS t/z 462 (MH+), 460 (M−H−).

WORKUP

后处理

  1. customChromatographic (30–40% ethyl acetate/hexane) purification