Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pyridine → 1-(2-Hexyl-4-tetradecylphenoxy)-3-(triphenylmethoxy)-2-propanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pyridine | HCID 1049 | — |
| 반응물 | Trityl chloride | HCID 6456 | — |
| 반응물 | 3-(2-Hexyl-4-tetradecylphenoxy)-1,2-propanediol | HCID 14819670 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | 1-(2-Hexyl-4-tetradecylphenoxy)-3-(triphenylmethoxy)-2-propanol | HCID 15030267 | 81.4% |
반응 단계
A mixture of 11.64 g of 3-(2-hexyl-4-tetradecylphenoxy)-1,2-propanediol, 12.32 g of trityl chloride and 40 ml of pyridine was stirred for 24 hours, then diluted with chloroform, washed with aqueous sodium bicarbonate, water, dried and the solvents evaporated under reduced pressure. The residue was coevaporated with toluene, giving 14.6 g of the desired compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04762942 |
| 출처 데이터셋 | uspto-grants-1988_08 |
| ORD ID | ord-d0aa0a5dc10f49cdb2798cea66321a25 |
| 출처 메모 | uspto-grants-1988_08 |