HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Phenyl-1-pentanol → HCID 69522656, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Phenyl-1-pentanol | HCID 61523 | — |
| Reactant | [5-(4-Fluorophenylcarbamoyl)pyrimidin-2-yloxy]acetic acid | HCID 21087356 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 69522656 | HCID 69522656 | 28% |
Reaction Steps
The titled compound was prepared from [5-(4-fluorophenylcarbamoyl)pyrimidin-2-yloxy]acetic acid using 5-phenyl-1-pentanol (56 mg, 0.34 mmol) as the coupling partner. Chromatography (gradient 5–95% ethyl acetate/hexane) through SiO2 yielded 6 mg (28%) of the titled compound. ESI-MS m/z 438 (MH+), 436 (M−H−).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07176310B1 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-896c36c41a2c4a078046d72b15346cc6 |
| Source note | uspto-grants-2007_02 |