Carbon Disulfide → HCID 178480415, compound

Participants

Reaction Steps

212 mg (0.845 mmol) of ((1-methylindole-3-yl)methyl)(2-aminophenyl)amine were dissolved in 1 ml of pyridine followed by the addition of 1 ml (16.9 mmol) of carbon disulfide and refluxing for 1 hour in a nitrogen atmosphere. The solvent was distilled off followed by purification by silica gel column chromatography (hexane:ethyl acetate=2:1) to obtain 96 mg of 1-((1-methylindole-3-yl)methyl)benzimidazole-2-thiol (yield: 39%).

Provenance & Evidence