HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21087563, compound → HCID 21087564, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21087563 | HCID 21087563 | — |
| Catalyst | Manganese dioxide | HCID 14801 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 21087564 | HCID 21087564 | 0.1% |
Reaction Steps
A solution of 9-ethyl-3-hydroxymethyl-6-methoxycarbazole (0.305 g, 1.2 mmol) in acetone (5 mL) was treated with MnO2 (0.52 g, 6 mmol) and the reaction stirred at room temperature for 60 hours. The reaction mixture was filtered and the solvent evaporated under reduced pressure. The crude was purified by column chromatography (heptane/ethyl acetate 5/1) to afford 0.190 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07176322B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-50a932ae424f4796823f5d18caf438eb |
| Source note | uspto-grants-2007_02 |