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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 348521Generated: October 29, 2026

HCID 21087563, compound → HCID 21087564, compound

https://huagongshe.com/reaction/348521

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 21087563HCID 21087563—
CatalystManganese dioxideHCID 14801—
SolventAcetoneHCID 180—
ProductHCID 21087564HCID 210875640.1%

Reaction Steps

A solution of 9-ethyl-3-hydroxymethyl-6-methoxycarbazole (0.305 g, 1.2 mmol) in acetone (5 mL) was treated with MnO2 (0.52 g, 6 mmol) and the reaction stirred at room temperature for 60 hours. The reaction mixture was filtered and the solvent evaporated under reduced pressure. The crude was purified by column chromatography (heptane/ethyl acetate 5/1) to afford 0.190 mg of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07176322B2
Source datasetuspto-grants-2007_02
ORD IDord-50a932ae424f4796823f5d18caf438eb
Source noteuspto-grants-2007_02