Silver Nitrate → HCID 178418580, compound

HRID 34894Notes

Reaction equation

HRID 34894 reaction equation
[NH:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[N:2]1.[N+]([O-])([O-])=O.[Ag+:14]>O>[NH:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[N:2]1.[Ag:14]

Participants

4

Reactant 2

HCID 24470Silver NitrateHCID 178418385HCID 178418385, compound

Product 1

HCID 178418580HCID 178418580, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

In 3,000 ml of water were dissolved 28 g of gelatin and 13.2 g of benzotriazole, and the solution was kept at 40° C. while stirring. To the solution was added 100 ml of an aqueous solution containing 17 g of silver nitrate over 2 minutes. Excess salts were sedimented and removed from the resulting emulsion by pH adjustment. Thereafter, the emulsion was adjusted to a pH of 6.30 to obtain a silver benzotriazole emulsion. The yield of the emulsion was 400 g.

Workup

  1. customwas kept at 40° C.
  2. customremoved from the resulting emulsion by pH adjustment

Sources & evidence

ORD record
ord-86168dd4db814de98319e1b2cb3e7425
Source dataset
uspto-grants-1988_08
Patent number
US04764451

Reaction notes

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