Acetophenone → 1-Phenylethanol, (S)-

Washed cicer arietinum L (bengal grams) 50 g. were taken into a conical flask and allowed to soak in deionised water (400 ml) for a period of 24 hr. Acetophenone (0.500 g; 0.004 moles) I(a) was added to the soaked cicer arietinum L (bengal grams) in the above water, covered and allowed to shake for 24 hr at room temperature (28° C). Then the green grams were filtered off and washed with deionised water (3×100 ml). The combined filtrate was extracted with chloroform (3×500 ml). The chloroform layer was dried and the crude product obtained (80 mg.). Pure 1-phenyl-(1S)-ethan-1-ol II(a) was obtained after column chromatography with silica gel using chloroform as eluent.

1. washWashed cicer arietinum L (bengal grams) 50 g
2. customwere taken into a conical flask
3. waitto shake for 24 hr at room temperature
4. custom(28° C)
5. filtrationThen the green grams were filtered off
6. washwashed with deionised water (3×100 ml)
7. extractionThe combined filtrate was extracted with chloroform (3×500 ml)
8. dry with materialThe chloroform layer was dried
9. customthe crude product obtained (80 mg.)

ORD record

ord-0146d0b903604c8a96b97cf6a3cd291d

Source dataset

uspto-grants-2007_02

DOI

10.6084/m9.figshare.5104873.v1

Patent number

US07179624B2