HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenamine, 2-phenoxy- → 1-Isothiocyanato-2-phenoxybenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenamine, 2-phenoxy- | HCID 75899 | — |
| Reactant | Thiocarbonyl diimidazole | HCID 11412697 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 1-Isothiocyanato-2-phenoxybenzene | HCID 22040439 | — |
Reaction Steps
1.96 g (0.011 mol) of thiocarbonyl diimidazole were added to a solution of 1.85 g (0.01 mol) of 2-phenoxyaniline in 50 ml of THF and the mixture was stirred at room temperature for 4 hours, giving, after removal of the solvent by distillation, the compound as a brown amorphous product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07179829B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-853bee71781a42c6a85dc3d3c78adb8d |
| Source note | uspto-grants-2007_02 |