3-Iodobenzonitrile → 5-(3-Iodophenyl)-2H-tetrazole

HRID 349448Notes

Reaction equation

HRID 349448 reaction equation
[I:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][CH:9]=1)[C:5]#[N:6].[NH:10]1C=N[N:12]=[N:11]1>>[I:1][C:2]1[CH:3]=[C:4]([C:5]2[N:10]=[N:11][NH:12][N:6]=2)[CH:7]=[CH:8][CH:9]=1

Participants

3

Reactant 2

HCID 1443413-IodobenzonitrileHCID 178418441HCID 178418441, compound

Product 1

HCID 445895335-(3-Iodophenyl)-2H-tetrazole

Procedure

The 3-iodobenzonitrile (3.6 g, 16.6 mmol) was converted to the corresponding tetrazole (4.1 g, 91%) utilizing reaction conditions previously described in Step (a) of example 1. CI-MS: C7H51N2 [M+1] 273.0.

Workup

  1. customreaction conditions

Sources & evidence

ORD record
ord-4396ed36665f41a78e5b47ec20ffb867
Source dataset
uspto-grants-2007_02
Patent number
US07179822B2

Reaction notes

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