HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromonicotinonitrile → 5-(5-Bromo-3-pyridyl)-1H-tetrazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromonicotinonitrile | HCID 736793 | — |
| Reactant | HCID 178418441 | HCID 178418441 | — |
| Product | 5-(5-Bromo-3-pyridyl)-1H-tetrazole | HCID 4173761 | — |
Reaction Steps
5-Bromo-nicotinonitrile (10.0 g, 55 mmol) was converted to the corresponding tetrazole (10.8 g, 75%) using the reaction conditions previously described in Step (a) of Example 1. 1H NMR (DMSO-d6) δ 9.17 (s, 1H), 8.89 (2, 1H), 8.59 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07179822B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-5dfb94800d034797aae1ccd04d6b2101 |
| Source note | uspto-grants-2007_02 |