HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylonitrile → 3-[(Cyclopropylmethyl)amino]propanenitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylonitrile | HCID 7855 | — |
| Reactant | Cyclopropanemethanamine | HCID 75646 | — |
| Product | 3-[(Cyclopropylmethyl)amino]propanenitrile | HCID 18348907 | — |
Reaction Steps
With stirring and cooling in an ice-bath to maintain a temperature of 8–10° C., acrylonitrile (0.614 ml) was added to aminomethylcyclopropane (0.651 g). The resultant mixture was stirred at room temperature for 15 h to give the title compound (1.02 g) as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07179835B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-b67c1ed0828f468a8f1f407676f3a4bf |
| Source note | uspto-grants-2007_02 |