HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic acid dihydrate → N-[1-(4-methylphenyl)-3-piperidinopropyl]quinaldinamide oxalate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic acid dihydrate | HCID 61373 | — |
| Reactant | N-[1-(4-methylphenyl)-3-piperidinopropyl]quinaldinamide | HCID 67930011 | — |
| Product | N-[1-(4-methylphenyl)-3-piperidinopropyl]quinaldinamide oxalate | HCID 67930072 | 80% |
Reaction Steps
The procedure of Example 7 was repeated using 917 mg (2.36 mmol.) of N-[1-(4-methylphenyl)-3-piperidinopropyl]quinaldinamide and 298 mg (2.36 mmol.) of oxalic acid dihydrate, to obtain 901 mg (yield: 80%) of the subject compound as a whilte crystalline product upon recrystallization from 8 ml of ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04764617 |
| Source dataset | uspto-grants-1988_08 |
| ORD ID | ord-d189332df8ad49bc8a8152b0d3067aa0 |
| Source note | uspto-grants-1988_08 |