HCID 11449317, compound → HCID 10171599, compound

HRID 350605Notes

Reaction equation

HRID 350605 reaction equation
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:11][NH:12][CH:13]2[CH2:18][CH2:17][C:16](=[O:19])[NH:15][C:14]2=[O:20])=[C:6]([NH:8][CH:9]=O)[CH:7]=1>O>[Cl:1][C:2]1[CH:7]=[C:6]2[C:5]([CH2:11][N:12]([CH:13]3[CH2:18][CH2:17][C:16](=[O:19])[NH:15][C:14]3=[O:20])[CH:9]=[N:8]2)=[CH:4][CH:3]=1

Participants

3

Reactant 1

HCID 11449317HCID 11449317, compound

Product 1

HCID 10171599HCID 10171599, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A solution of 0.20 g of the product from stage 5 in 10 ml of distilled water was stirred for 72 hours at 20° C. The mixture was then filtered, the filtrate was concentrated by evaporation in vacuo, and the residue was dried. 0.13 g (68% of theory) of the title compound was obtained as a white solid.

Workup

  1. filtrationThe mixture was then filtered
  2. concentrationthe filtrate was concentrated by evaporation in vacuo
  3. customthe residue was dried

Sources & evidence

ORD record
ord-008ea9f54ccb4622a2fc93d97910b9fc
Source dataset
uspto-grants-2007_02
Patent number
US07183274B2

Reaction notes

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