HCID 18762647, compound → HCID 10125239, compound

HRID 350607Notes

Reaction equation

HRID 350607 reaction equation
[O:1]=[C:2]1[CH:7]([NH:8][CH2:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=2[NH:16][CH:17]=O)[CH2:6][CH2:5][C:4](=[O:19])[NH:3]1>O>[N:16]1[C:11]2[C:10](=[CH:15][CH:14]=[CH:13][CH:12]=2)[CH2:9][N:8]([CH:7]2[CH2:6][CH2:5][C:4](=[O:19])[NH:3][C:2]2=[O:1])[CH:17]=1

Participants

3

Reactant 1

HCID 18762647HCID 18762647, compound

Product 1

HCID 10125239HCID 10125239, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A solution of 0.91 g of the product from stage 2 in 5 ml of distilled water was stirred for 24 hours at 20° C. The reaction solution was then evaporated to dryness in vacuo. The remaining solid was triturated with diethyl ether, 0.85 g (99% of theory) of the title compound remaining as a yellow powder.

Workup

  1. customThe reaction solution was then evaporated to dryness in vacuo
  2. customThe remaining solid was triturated with diethyl ether, 0.85 g (99% of theory) of the title compound

Sources & evidence

ORD record
ord-8487f041be854d1692dd2c9bab373d66
Source dataset
uspto-grants-2007_02
Patent number
US07183274B2

Reaction notes

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