HRID350656

反应详情

EQUATION

反应方程式

HRID 350656 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Methyl 3-benzyloxy-6-methoxy-picolinate (20 mg) was dissolved in 1 ml of methanol. A 1 N aqueous sodium hydroxide solution (0.33 ml) was added to the solution, and a reaction was allowed to proceed at room temperature for 3 hr. The reaction solution was then adjusted to pH 3 by the addition of 1 N hydrochloric acid. The precipitate was collected by filtration to give 12 mg (yield 63%) of the title compound.

WORKUP

后处理

  1. filtrationThe precipitate was collected by filtration