HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 1-(4-Aminophenyl)-6-methylsulfanyl-2,3,4,5-tetrahydropyridinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 1-(4-Aminophenyl)piperidine-2-thione | HCID 12114408 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 1-(4-Aminophenyl)-6-methylsulfanyl-2,3,4,5-tetrahydropyridinium iodide | HCID 12114409 | — |
Reaction Steps
1.25 ml (20.0 mmol) of iodomethane are added to a solution of 3.74 g (18.1 mmol) of 1-(4-aminophenyl)piperidine-2-thione in 30 ml of acetone, and the mixture is stirred at room temperature for 48 hours. The reaction mixture is evaporated, giving 1-(4-aminophenyl)-6-methylsulfanyl-2,3,4,5-tetrahydropyridinium iodide as a brownish solid; ESI 221.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07183277B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-ab13e872e5be472ba7cd1ae421525626 |
| Source note | uspto-grants-2007_02 |